Open main menu
Home
Random
Recent changes
Special pages
Community portal
Preferences
About Wikipedia
Disclaimers
Incubator escapee wiki
Search
User menu
Talk
Dark mode
Contributions
Create account
Log in
Editing
Polyimide
(section)
Warning:
You are not logged in. Your IP address will be publicly visible if you make any edits. If you
log in
or
create an account
, your edits will be attributed to your username, along with other benefits.
Anti-spam check. Do
not
fill this in!
===Analysis=== The imidization reaction can be followed via [[Infrared spectroscopy|IR spectroscopy]]. The IR spectrum is characterized during the reaction by the disappearance of absorption bands of the poly(amic acid) at 3400 to 2700 cm<sup>β1</sup> (OH stretch), ~1720 and 1660 (amide C=O) and ~1535 cm<sup>β1</sup> (C-N stretch). At the same time, the appearance of the characteristic imide bands can be observed, at ~1780 (C=O asymm), ~1720 (C=O symm), ~1360 (C-N stretch) and ~1160 and 745 cm<sup>β1</sup> (imide ring deformation).<ref>K. Faghihi, J. Appl. Polym. Sci., 2006, 102, 5062β5071. Y. Kung and S. Hsiao, J. Mater. Chem., 2011, 1746β1754. L. Burakowski, M. Leali and M. Angelo, Mater. Res., 2010, 13, 245β252.</ref>β γDetailed analyses of polyimide<ref>{{Cite journal |last1=Kato |first1=Tomofumi |last2=Yamada |first2=Yasuhiro |last3=Nishikawa |first3=Yasushi |last4=Ishikawa |first4=Hiroki |last5=Sato |first5=Satoshi |date=2021-06-30 |title=Carbonization mechanisms of polyimide: Methodology to analyze carbon materials with nitrogen, oxygen, pentagons, and heptagons |url=https://www.sciencedirect.com/science/article/pii/S0008622321002839 |journal=Carbon |language=en |volume=178 |pages=58β80 |doi=10.1016/j.carbon.2021.02.090 |s2cid=233539984 |issn=0008-6223|url-access=subscription }}</ref> and carbonized polyimide<ref>{{Cite journal |last1=Kato |first1=Tomofumi |last2=Yamada |first2=Yasuhiro |last3=Nishikawa |first3=Yasushi |last4=Ishikawa |first4=Hiroki |last5=Sato |first5=Satoshi |date=2021-06-30 |title=Carbonization mechanisms of polyimide: Methodology to analyze carbon materials with nitrogen, oxygen, pentagons, and heptagons |url=https://www.sciencedirect.com/science/article/pii/S0008622321002839 |journal=Carbon |language=en |volume=178 |pages=58β80 |doi=10.1016/j.carbon.2021.02.090 |s2cid=233539984 |issn=0008-6223|url-access=subscription }}</ref> and graphitized polyimide<ref>{{Cite journal |last1=Kato |first1=Tomofumi |last2=Yamada |first2=Yasuhiro |last3=Nishikawa |first3=Yasushi |last4=Otomo |first4=Toshiya |last5=Sato |first5=Hayato |last6=Sato |first6=Satoshi |date=2021-10-01 |title=Origins of peaks of graphitic and pyrrolic nitrogen in N1s X-ray photoelectron spectra of carbon materials: quaternary nitrogen, tertiary amine, or secondary amine? |journal=Journal of Materials Science |language=en |volume=56 |issue=28 |pages=15798β15811 |doi=10.1007/s10853-021-06283-5 |bibcode=2021JMatS..5615798K |s2cid=235793266 |issn=1573-4803|doi-access=free }}</ref> have been reported.
Edit summary
(Briefly describe your changes)
By publishing changes, you agree to the
Terms of Use
, and you irrevocably agree to release your contribution under the
CC BY-SA 4.0 License
and the
GFDL
. You agree that a hyperlink or URL is sufficient attribution under the Creative Commons license.
Cancel
Editing help
(opens in new window)